Skip to main content

Featured Project 03

Silicon Microfluidics

Cavitation-on-Chip Microfluidic Reactor

An eight-orifice silicon–glass reactor engineered to trigger cavitation at reduced inlet pressure and produce several distinct two-phase flow regimes on a single chip.

My Role

Device co-development · Experimental testing · High-speed imaging · Flow analysis

First author · Physics of Fluids · 2021

I co-developed the eight-orifice device and led the experimental testing, high-speed flow imaging, and flow-regime analysis presented in this work.

Scanning-electron micrographs of the eight-orifice device, the engineered orifice roughness, and high-speed imaging of the resulting cavitating jets.

Scanning-electron micrographs of the eight-orifice device, the engineered orifice roughness, and high-speed imaging of the resulting cavitating jets.

8

Parallel micro-orifices

2.24 MPa

Cavitation inception pressure

≈46%

Reduction vs. reference geometry

7,000 fps

High-speed imaging frame rate

01 — The Engineering Challenge

Trigger cavitation sooner. Unlock more flow regimes.

The objective was to initiate hydrodynamic cavitation at a lower upstream pressure than a conventional single-orifice geometry, while giving a single chip access to several distinct two-phase flow patterns.

01 · Lower the threshold

Reduce the pressure needed to initiate cavitation.

A single-orifice reference geometry required 4.13 MPa of upstream pressure before cavitation would begin.

02 · Expand flow diversity

Produce multiple distinct flow regimes from a single chip.

Flow morphology needed to change without adjusting the external operating conditions.

Line diagrams of four two-phase flow regimes observed downstream of the orifices: bubbly flow, twin cavities, cloud jet, and sheet cavity.

The Target

Initiate cavitation at a lower pressure while producing several useful flow regimes on one chip.

02 — Eight-Orifice Reactor Architecture

One inlet, split eight ways.

Flow entered through a single expanding chamber that divided into eight parallel micro-orifices before recombining in a shared extension zone. The inlet geometry set the velocity distribution across the array, while engineered sidewall roughness gave each channel a repeatable nucleation site.

Schematic of the eight-orifice reactor: a single inlet chamber divides into eight parallel micro-orifices labeled 01 through 08, which discharge into a shared extension zone and recombine into two common outlets.
Detail schematic of a single micro-orifice cross-section, 300 micrometers wide and 1000 micrometers long, with triangular roughness features engineered along half the channel length on each sidewall.

01  Parallelization

Eight parallel branches multiply the number of active cavitation sites within a single compact reactor.

02  Functional sidewalls

Triangular sidewall features, evenly spaced along each channel, promote heterogeneous nucleation at the walls.

03  Geometry-shaped distribution

The expanding entrance geometry produces channel-to-channel velocity variation even under a single inlet pressure.

8

Parallel orifices

300 µm

Orifice width

1000 µm

Orifice length

50 µm

Channel depth

03 — From Geometry to a Silicon–Glass Device

Silicon etched. Stress managed. Chip sealed.

The eight-orifice layout became a closed microreactor through oxide masking, deep silicon etching, and backside stress control, sealed by anodic bonding to glass and integrated into a five-port fluidic package.

Silicon block with a patterned oxide layer on top, showing eight rectangular mask openings arranged in two rows.
01

Oxide Hard Mask

250 µm Si · 500 nm SiO₂

Cross-section of silicon with three deep trenches etched through the oxide mask, each sidewall patterned with triangular roughness features.
02

Deep Silicon Etch

Deep reactive-ion etching transferred the channel geometry and engineered sidewalls into the silicon.

Cross-section of the silicon stack showing a thin titanium layer and a thicker aluminum layer applied to the backside.
03

Stress Management

A 10 nm Ti + 2 µm Al backside coating reduced fracture risk during processing.

Silicon block with four circular ports drilled through, viewed from above at an angle.
04

Port Opening + Clean

Inlet, outlet, and pressure ports were opened, and temporary protective films were stripped.

Exploded view of a glass lid aligned above the silicon block with four ports, joined by an applied electric field during anodic bonding.
05

Anodic Bonding

A Borofloat-33 glass lid was anodically bonded to seal the silicon channels.

Finished chip mounted in a five-port fluidic holder with tubing connected at each port.
06

Fluidic Packaging

A five-port holder provided external flow connections and in-line pressure measurement.

Collaborative Fabrication

The silicon micromachining, anodic bonding, and fluidic packaging shown here were executed by the broader project team.

I collaborated on the device geometry and then led the experimental program that followed.

04 — Experimental Characterization

Imaging cavitation at 7,000 frames per second.

A pressure-driven test rig paired controlled flow, the packaged silicon–glass device, back illumination, and high-speed imaging to resolve transient two-phase behavior.

My roleSetup operation · High-speed imaging · Quantitative analysis

Photograph of the experimental rig: a pressurized gas cylinder and flow regulator feed the packaged silicon–glass reactor, illuminated from behind and imaged through a high-speed camera; inset shows a captured high-speed frame of cavitating flow inside one channel.
Pressurized gas cylinder with a mechanical gauge and regulating valve.

Pressure source

Digital flow regulator displaying an inlet pressure of 2.24 MPa.

Flow control

Cylindrical back-illumination light source with a diffused white lens face.

Back illumination

Packaged silicon–glass reactor chip with a visible channel window and threaded fluidic ports.

Packaged reactor

High-speed camera with a macro lens aimed at the reactor.

High-speed camera

7,000 fps

Frame rate

1 µs

Exposure time

2.24 MPa

Cavitation inception

05 — Mapping Cavitation Behaviour

From raw frames to a flow-regime map.

My Role

High-speed imaging · Frame analysis · Flow-pattern classification · Quantitative interpretation

High-speed image sequences were analyzed to detect cavitation inception, classify the evolving flow regime, and quantify vapor development across all eight parallel micro-orifices.

01Detect Inception
02Classify Regimes
03Quantify Vapor
04Map Behaviour
High-speed frames of the eight-orifice array showing cavitation first appearing at micro-orifices 3 and 6, with magnified insets marked (a) 2.24 MPa and (b) 2.29 MPa.
Annotated high-speed frame spanning channels 2 through 4, marking cavitation inception, cavitating flow, circulated bubbly flow, vapor cloud jet flow, and a single sheet vapor cavity.
Three frame-by-frame void-fraction maps, color-coded by volume fraction, showing vapor and vapor-cloud regions against the surrounding fluid.
Chart mapping the classified flow regime for each of the eight channels against upstream pressure and cavitation number, from non-cavitating flow to a fully developed cavity.
Frames
Segment vapor
Compute void fraction
Classify regime
Align with pressure

7,000 fps

High-speed capture

8 channels

Parallel comparison

Frame by frame

Void-fraction analysis

06 — Results & Engineering Takeaways

Lower pressure.More useful flow states.

The eight-orifice reactor reached cavitation inception at 2.24 MPa—approximately 46% below the 4.13 MPa single-orifice reference—while supporting several cavitation patterns under the same operating condition.

2.24MPa

Cavitation inception

4.13 MPa

Referenced single-orifice design

2.24 MPa

Eight-orifice reactor

≈46%

Lower

Published pressure response

1.52.02.53.03.54.04.55.06.06.57.07.58.0Upstream pressure (MPa)Cavitation numberCavitation inception

Source: Published high-speed study of cavitation inception in micro-orifices (data reproduced).

From sheet cavity to fully developed flow

High-speed frame of a roughened micro-orifice channel showing a continuous vapor sheet along the sidewall.

Sheet cavity

High-speed frame showing the vapor sheet breaking into an unsteady, oscillating cavitating flow downstream of the orifice.

Fully developed oscillating flow

High-speed frame showing a mix of circular and non-circular bubbles downstream of the orifice.

Downstream bubble morphology

01

Earlier nucleation

Engineered sidewall roughness promoted cavitation at a lower upstream pressure.

02

Parallel functionality

Eight micro-orifices supported distinct cavitation behaviours within one device.

03

Evidence-led design

High-speed imaging connected pressure conditions to evolving vapor structures.

My ContributionCo-developed the concept and geometry · Led experimental characterization · Analyzed the flow behaviour · Led interpretation and writing